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This invention relates to a method of producing a green body, which is subsequently sintered, by means of a cementation or a sintering material, having a high content of a particular zeolite, of a particular silica sol and of a colloidal silica.
The silica sols from which the sintering materials can be derived are generally characterized by a water content of less than 10%. The maximum water contents are defined by the conditions and the process selected. These can be as follows:
1. The silica sol can be produced by the neutralization of a hydrolyzable silicate with a base and subsequently heating the sol to a temperature of 140.degree. to 200.degree. C. The sol is subsequently acidified and the water precipitated. The sol is dried at 100.degree.-150.degree. C. and is then spray dried or treated in an evaporator.
2. As a second production method, the silica sol can be produced by the hydrolysis of a chlorosilane and, subsequently, by the addition of a base, which results in the precipitation of the product.
A third production method is the neutralization of an organosilicon compound of the general formula (RO).sub.3 Si–Si(OR).sub.3 with an alkali hydroxide. By treating the reaction product, the silica sol precipitates as the alkali hydroxide counter ion is incorporated in the lattice of the oxosilicon. This method is characterized by the excellent reproducibility of the product.
In order to achieve small grain sizes of the silica sols, that is to say of from 1 to 3.mu.m, it is advantageous to use spray drying methods, the sols being dried with one or more ventilating nozzles.
The spray drying methods result in the formation of small crystallites. The surface of these crystallites is characterized by a high level of active sites. A large part of the active sites are however destroyed by attack from the surrounding atmosphere
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